dc.contributor.author |
Rathod, Chirag H. |
|
dc.contributor.author |
Patel, Anilkumar S. |
|
dc.date.accessioned |
2024-11-15T07:57:22Z |
|
dc.date.available |
2024-11-15T07:57:22Z |
|
dc.date.issued |
2021 |
|
dc.identifier.citation |
Rathod, C. H., & Patel, A. S. (2021). Synthesis of Pyrrole Derivatives via Cycloaddition Reaction of Reissert Hydrofluoroborate Salts with α-Bromoacrylamides. Analytical Chemistry Letters, 11(3), 289-302. |
en_US |
dc.identifier.uri |
http://10.9.150.37:8080/dspace//handle/atmiyauni/1534 |
|
dc.description.abstract |
Abstract
An investigation of α-bromoacrylamide as a dienophile for the cycloaddition reaction of Reissert hydrofluoroborate salt of quinoline/phenanthridine has been carried out. The optimized condition has been developed for the [4+2] cycloaddition reaction of Reissert hydrofluroborate salt and α-bromoacrylamide by using K2CO3 in DMF under moderate temperature to afford highly functionalized pyrrole derivatives (6a-f and 7a-f) in very good to excellent yield. The structures of newly synthesized compounds were established based on FT-IR, Mass, 1H and 13C NMR spectral techniques. Besides, the structure of compound 7a has been confirmed by 2D NMR experiments (COSY and HSQC). |
en_US |
dc.language.iso |
en |
en_US |
dc.publisher |
Analytical Chemistry Letters |
en_US |
dc.title |
Synthesis of Pyrrole Derivatives via Cycloaddition Reaction of Reissert Hydrofluoroborate Salts with α-Bromoacrylamides |
en_US |
dc.type |
Article |
en_US |