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Synthesis, characterization, crystal, and molecular structure analysis of 3,4- dihydro-6-(2-hydroxyphenyl)-5-nitro-4- phenylpyrimidin-2(1H)-one
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| dc.contributor.author | Savant, M.M. | |
| dc.contributor.author | Gowda, L.B. | |
| dc.contributor.author | Anandalwar, S.M. | |
| dc.contributor.author | Prasad, J.S. | |
| dc.contributor.author | Shah, A. | |
| dc.contributor.author | Naliapara, Y.T. | |
| dc.date.accessioned | 2023-05-17T02:12:43Z | |
| dc.date.available | 2023-05-17T02:12:43Z | |
| dc.date.issued | 2015-04-11 | |
| dc.identifier.citation | M. M. Savant, L. B. Gowda, S. M. Anandalwar, J. S. Prasad, A. Shah & Y. T. Naliapara (2015) Synthesis, Characterization, Crystal, and Molecular Structure Analysis of 3,4- dihydro-6-(2-hydroxyphenyl)-5-nitro-4-phenylpyrimidin-2(1H)-one, Molecular Crystals and Liquid Crystals, 609:1, 118-125, DOI: 10.1080/15421406.2014.928425 | en_US |
| dc.identifier.issn | 1563-5287 | |
| dc.identifier.uri | http://10.9.150.37:8080/dspace//handle/atmiyauni/972 | |
| dc.description | The authors are thankful to FIST-DST, SAP-UGC for their generous financial and instrumentation support. Special thanks are due to “National Facility for Drug Discovery through New Chemical Entities Development & Instrumentation Support to Small Manufacturing Pharma Enterprises” Programme under Drug & Pharma Research Support jointly funded by DST & Government of Gujarat Industries Commissionerate. Government of India project SP/I2/FOO/93 and University of Mysore, Mysore for financial assistance. | en_US |
| dc.description.abstract | A novel nitro and 2-hydroxyphenyl functionalized pyrimidinone at C5 and C6, respectively, has been synthesized using 1-(2-hydroxyphenyl)-2-nitroethanone, benzaldehyde, urea, and etidronic acid as a catalyst is described. The synthesized compound characterized by spectroscopic techniques and finally confirmed by X-ray diffraction studies. The molecule crystallizes in the monoclinic crystal class in the space group P21/c with cell parameters a = 11.1070(10)Å, b = 8.8210(4)Å, c = 15.1110(13)Å, β = 106.193(2)◦, and Z = 4. The pyrimidine ring adopts flattened boat conformation. | en_US |
| dc.language.iso | en | en_US |
| dc.publisher | Molecular Crystals and Liquid Crystals | en_US |
| dc.subject | Flat boat | en_US |
| dc.subject | hydrogen bonds | en_US |
| dc.subject | multicomponent | en_US |
| dc.subject | nitro-dihydropyrimidine | en_US |
| dc.subject | Polymeric chains | en_US |
| dc.title | Synthesis, characterization, crystal, and molecular structure analysis of 3,4- dihydro-6-(2-hydroxyphenyl)-5-nitro-4- phenylpyrimidin-2(1H)-one | en_US |
| dc.type | Article | en_US |
